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Articles
X-ray Diffraction: New High-Speed Technique Based on X-ray Spectrography
1 Department of Metallurgy and Material Science, Massachusetts Institute of Technology, Cambridge 02139
A method has been developed for obtaining lattice spacings of powder samples by x-ray diffraction in times potentially as short as 1 second. The sample is irradiated with polychromatic radiation from an x-ray tube, and the energy spectrum of x-rays scattered at a given angle is observed with a semiconductor radiation detector, coupled with a pulse-height analyzer.
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Science. ISSN 0036-8075 (print), 1095-9203 (online)